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Casanova and B. Waegell, Bull. chim. France, 1975,598. T. C. Clarke, L. A. Wendling, and R. G. Bergman, J . Amer. Chem. , 1975,97, 5638. 5% retention of optical purity, and predominantly doubly inverted) and (123) in nearly racemic form. 6% optical purity, and predominantly double retention of configuration). With the singly deuteriated analogues, (121) exhibits a deuterium isotope effect of about 10% on the optical purity of the products, while a real, but somewhat smaller, effect is observed with (122).
Abramova, Izvest. Akad. Nauk. , Ser. , 1975, 1912, (Chem. , 1975, 83,192 625); E. Miiller, Chem. , 1975,108,1394,1401; V. A. Razin, M. V. Eremenks, and K. A. Oglobin, Zhur. org. , 1975,11,2439 (Chem. , 1976,84,58 700). T. Hiyama, H. Koide, and H. Nozaki, Bull. Chem. Japan, 1975,48,2918. G. Mehta and B. P. Singh, Tetrahedron Letters, 1975,4498; H. M. Campbell, P. A. Gunn, A. J. McAlees, and R. McCrindle, Canad. J . , 1975,53,20. 5 % CMe, MeOCMe, CH = CH C Me, OMe f-- Me '"~gOAr Me Me Scheme 30 PhCH=CHCHO B:H2 HgOAc +- PhCH=CHCH=NH + Reagents: i, Pb(OAc), Scheme 31 - CMe, Me tAigOAc 82 % Reagents: i.
Bagratuni, and Sh. Badanyan, Armyan. , 1975,28,281 (Chem. , 1975,83, 78 666). R R. Kostikov and A. P. Molchanov, Zhur. org. , 1975,83,147 155). Sato, T. Tanaka, J. Tsunetsugu, and S. Ebine, Bull. Chem. SOC. Japan, 1975,58,2395. J. D. White and L. G. Wade, J . Org. , 1975,40,118. G. Neumann, and P. Weyerstahl, Annalen, 1975,201. 20 AIicyclic Chemistry (69) 45 % overall Reagents: i, :CX,;ii, AgBF,; iii, LiCl-DMF Scheme 10 positions of phenanthrene (73) survives chromatographic separation. This particular dibenzonorcaradiene is remarkably stable, and can be cleaved only under drastic conditions.